One‐Pot Catalyst‐Free Synthesis of β‐ and γ‐Hydroxy Sulfides Using Diaryliodonium Salts and Microwave Irradiation | Zendy

Vaddula Buchi Reddy | Zendy; Varma Rajender S. | Zendy; Leazer John | Zendy

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One‐Pot Catalyst‐Free Synthesis of β‐ and γ‐Hydroxy Sulfides Using Diaryliodonium Salts and Microwave Irradiation

Author(s) -

Vaddula Buchi Reddy,

Varma Rajender S.,

Leazer John

Publication year - 2012

Publication title -

european journal of organic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.825

H-Index - 155

eISSN - 1099-0690

pISSN - 1434-193X

DOI - 10.1002/ejoc.201201313

Subject(s) - chemistry , ethylene glycol , microwave irradiation , catalysis , potassium thiocyanate , thiocyanate , solvent , organic chemistry , base (topology) , combinatorial chemistry , mathematical analysis , mathematics

A simple and rapid one‐pot protocol is described for the preparation of α‐ and β‐hydroxy sulfides. The direct solvent‐free microwave irradiation of diaryliodonium salts, potassium thiocyanate, and ethylene glycol/β‐propylene glycol without any catalyst or base affords the final compounds in good yields (65–95 %) in around 10–25 min.

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