The Overcrowded Borazine Derivative of Hexabenzotriphenylene Obtained through Dehydrohalogenation | Zendy

Biswas Sunanda | Zendy; Müller Matthias | Zendy; Tönshoff Christina | Zendy; Eichele Klaus | Zendy; MaichleMössmer Cäcilia | Zendy; Ruff Adrian | Zendy; Speiser Bernd | Zendy; Bettinger Holger F. | Zendy

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The Overcrowded Borazine Derivative of Hexabenzotriphenylene Obtained through Dehydrohalogenation

Author(s) -

Biswas Sunanda,

Müller Matthias,

Tönshoff Christina,

Eichele Klaus,

MaichleMössmer Cäcilia,

Ruff Adrian,

Speiser Bernd,

Bettinger Holger F.

Publication year - 2012

Publication title -

european journal of organic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.825

H-Index - 155

eISSN - 1099-0690

pISSN - 1434-193X

DOI - 10.1002/ejoc.201200322

Subject(s) - dehydrohalogenation , chemistry , borazine , trimer , tetramer , derivative (finance) , organic chemistry , stereochemistry , dimer , catalysis , boron nitride , financial economics , economics , enzyme

Treatment of 9‐chloro‐9‐bora‐10‐azaphenanthrene with potassium hexamethyldisilazide yields the borazine derivative of hexabenzotriphenylene ( 4 ). This compound, the formal trimer of 9,10‐azaboraphenanthryne ( 6 ), is soluble in organic solvents and was fully characterized. The tetramer of 6 is formed as a byproduct in the previously described high‐temperature synthesis of 4 .

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