Methanofullerenes from Macrocyclic Malonates | Zendy

Carano Maurizio | Zendy; Corvaja Carlo | Zendy; Garlaschelli Luigi | Zendy; Maggini Michele | Zendy; Marcaccio Massimo | Zendy; Paolucci Francesco | Zendy; Pasini Dario | Zendy; Righetti Pier Paolo | Zendy; Sartori Elena | Zendy; Toffoletti Antonio | Zendy

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Methanofullerenes from Macrocyclic Malonates

Author(s) -

Carano Maurizio,

Corvaja Carlo,

Garlaschelli Luigi,

Maggini Michele,

Marcaccio Massimo,

Paolucci Francesco,

Pasini Dario,

Righetti Pier Paolo,

Sartori Elena,

Toffoletti Antonio

Publication year - 2003

Publication title -

european journal of organic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.825

H-Index - 155

eISSN - 1099-0690

pISSN - 1434-193X

DOI - 10.1002/ejoc.200390044

Subject(s) - chemistry , malonate , moiety , supramolecular chemistry , crown ether , electrochemistry , electron paramagnetic resonance , molecule , alkyl , polymer chemistry , mass spectrometry , combinatorial chemistry , ion , organic chemistry , physics , electrode , nuclear magnetic resonance , chromatography

In this paper we describe the synthesis and intercomparison of several new methanofullerenes, each bearing a macrocyclic crown ether containing a malonate moiety directly attached to the C 60 ‐fullerene core. Their complexing abilities with primary alkylammonium ions were investigated by NMR and mass spectrometry, and also by transport experiments through a liquid membrane. We also report on their electrochemical behaviour, together with EPR analysis of their supramolecular complexes with alkyl ammonium molecules labelled with a stable nitroxide radical. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2003)

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