Very Rapid Preparation of SmI 2  by Sonic Treatment of Iodoform and Metallic Samarium | Zendy

Concellón José M. | Zendy; RodríguezSolla Humberto | Zendy; Bardales Eva | Zendy; Huerta Mónica | Zendy

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Very Rapid Preparation of SmI 2 by Sonic Treatment of Iodoform and Metallic Samarium

Author(s) -

Concellón José M.,

RodríguezSolla Humberto,

Bardales Eva,

Huerta Mónica

Publication year - 2003

Publication title -

european journal of organic chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.825

H-Index - 155

eISSN - 1099-0690

pISSN - 1434-193X

DOI - 10.1002/ejoc.200210669

Subject(s) - iodoform , samarium , diiodomethane , chemistry , sonication , iodine , metal , nuclear chemistry , heptanal , inorganic chemistry , organic chemistry , chromatography , catalysis , aldehyde , surface energy

A very rapid preparation of SmI 2 by sonication of a mixture of metallic samarium and iodoform in THF is described. To prove the synthetic applications of the obtained SmI 2 several high‐yielding reactions were carried out. Preliminary results for the generation of SmI 2 in THF by sonication from diiodomethane, 1,2‐diiodoethane, or iodine are also described. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2003)

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