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Synthesis and Structure of New Macrocycles Including Spiro‐1,3‐Dioxane Units
Author(s) -
Grosu Ion,
Bogdan Elena,
Plé Gérard,
Toupet Loïc,
Ramondenc Yvan,
Condamine Eric,
PeulonAgasse Valérie,
Balog Mirela
Publication year - 2003
Publication title -
european journal of organic chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.825
H-Index - 155
eISSN - 1099-0690
pISSN - 1434-193X
DOI - 10.1002/ejoc.200200615
Subject(s) - chemistry , monomer , mass spectrometry , solid state , mass spectrum , nuclear magnetic resonance spectroscopy , stereochemistry , combinatorial chemistry , polymer chemistry , organic chemistry , polymer , chromatography
The efficient synthesis of new macrocycles — “monomers” and “dimers” — containing spiro‐1,3‐dioxane units is reported. The structure of the compounds was determined from high‐field NMR spectra, FAB and MALDI + mass spectrometry investigations. The solid‐state molecular structures of three compounds was determined. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2003)