Tin‐Mediated Route to Polytungstates of Rh II  and Pd II | Zendy

Sokolov Maxim N. | Zendy; Kalinina Irina V. | Zendy; Peresypkina Eugenia V. | Zendy; Moroz Nikolay K. | Zendy; Naumov Dmitry Yu. | Zendy; Fedin Vladimir P. | Zendy

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Tin‐Mediated Route to Polytungstates of Rh II and Pd II

Author(s) -

Sokolov Maxim N.,

Kalinina Irina V.,

Peresypkina Eugenia V.,

Moroz Nikolay K.,

Naumov Dmitry Yu.,

Fedin Vladimir P.

Publication year - 2013

Publication title -

european journal of inorganic chemistry

Language(s) - Slovenian

Resource type - Journals

SCImago Journal Rank - 0.667

H-Index - 136

eISSN - 1099-0682

pISSN - 1434-1948

DOI - 10.1002/ejic.201201162

Subject(s) - chemistry , thermogravimetric analysis , tin , spectroscopy , rhodium , nuclear magnetic resonance spectroscopy , crystallography , nuclear chemistry , stereochemistry , catalysis , organic chemistry , physics , quantum mechanics

Three polyoxotungstates of Sn II , Pd II , and Rh II , Na 8 [H 2 SnW 12 O 42 ] · n H 2 O [ 1 , n = 22.75 ( 1a ) and n = 31.10 ( 1b )], Na 2 K(H)[Pd(H 2 O) 4 ][H 2 W 12 O 48 {Pd(H 2 O) 3 } 2 ] · 10H 2 O ( 2 ), and Na 8 [Rh 2 (H 2 O) 2 (W 5 O 18 ) 2 ] · 21.25H 2 O ( 3 ) were obtained. The complexes were characterized by X‐ray analysis, solid‐state 1 H NMR spectroscopy, IR spectroscopy, thermogravimetric analysis, and elemental analysis.

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