Organocatalyzed Epoxidation of Alkenes in Continuous Flow using a Multi‐Jet Oscillating Disk Reactor | Zendy

Spaccini Raffaele | Zendy; Liguori Lucia | Zendy; Punta Carlo | Zendy; Bjørsvik HansRené | Zendy

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Organocatalyzed Epoxidation of Alkenes in Continuous Flow using a Multi‐Jet Oscillating Disk Reactor

Author(s) -

Spaccini Raffaele,

Liguori Lucia,

Punta Carlo,

Bjørsvik HansRené

Publication year - 2012

Publication title -

chemsuschem

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 2.412

H-Index - 157

eISSN - 1864-564X

pISSN - 1864-5631

DOI - 10.1002/cssc.201100262

Subject(s) - continuous reactor , residence time (fluid dynamics) , continuous flow , batch reactor , flow chemistry , jet (fluid) , flow (mathematics) , chemistry , plug flow reactor model , microreactor , mixing (physics) , chemical engineering , continuous stirred tank reactor , catalysis , materials science , organic chemistry , mechanics , physics , geotechnical engineering , quantum mechanics , engineering

The times are changing: A batch process, the Minisci epoxidation, is transformed into a continuous‐flow protocol for the selective aerobic radical epoxidation of alkenes. The use of a novel reactor type allows to considerably shorten reactor residence times. Experimental results suggest that two different reaction mechanisms exist for the oxidation: one for the batch conditions and a different one for flow synthesis protocol.

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