Crystal Structure of Fibrillar Sodium Trimolybdate Hydrate by Powder Diffraction Method | Zendy

Łasocha W. | Zendy; RafalskaŁasocha A. | Zendy; Schenk H. | Zendy

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Crystal Structure of Fibrillar Sodium Trimolybdate Hydrate by Powder Diffraction Method

Author(s) -

Łasocha W.,

RafalskaŁasocha A.,

Schenk H.

Publication year - 1997

Publication title -

crystal research and technology

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.377

H-Index - 64

eISSN - 1521-4079

pISSN - 0232-1300

DOI - 10.1002/crat.2170320412

Subject(s) - hydrate , crystallography , crystal structure , crystallite , rietveld refinement , polyhedron , powder diffraction , ab initio , chemistry , diffraction , sodium , materials science , mathematics , physics , geometry , optics , organic chemistry

The crystal structure of polycrystalline fibrillar sodium trimolybdate Na 2 Mo 3 O 10 . 3 H 2 O, has been solved ab initio by Powder Diffraction – Direct Methods package POWSIM. The structure was refined by the Rietveld method with final discrepancy factors R F = 6.9 and R wp = 17.1%. The structure consists of polymeric chains of Mo‐O polyhedra parallel to the b axis. The space group is C2/m (12), a = 17.179(1), b = 3.7757(3), c = 10.8571(8) Å, β = 115.417(6)°, V = 636.06(6) Å 3 , Z = 2.

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