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Rietveld Refinement of the Crystal Structure of Nickel Hexaamina Perchlorate and ‐Tetrafluorborate
Author(s) -
LutoslawskaRogóż J.,
Mucha D.,
Hodorowicz S. A.
Publication year - 1996
Publication title -
crystal research and technology
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.377
H-Index - 64
eISSN - 1521-4079
pISSN - 0232-1300
DOI - 10.1002/crat.2170310406
Subject(s) - perchlorate , nickel , rietveld refinement , crystal structure , crystallography , chemistry , crystal (programming language) , materials science , ion , computer science , organic chemistry , programming language
Room‐temperature phases of nickel hexamina perchlorate (NHP) and nickel hexaamina tetrafluorborate (NHT) were analysed by means of X‐ray powder diffractometry. Both compounds crystallize in the cubic system (Fm 3 m space group) with cell parameters: a = 11.4689 Å for NHP and a = 11.2692 Å for NHT structure, respectively. The crystal structures of these compounds were refined using Rietveld method.