1 H‐NMR and IR Investigations of Phase Situation in Solid Sodium‐Tetramethylammonium Decamolybdate 3.5‐Hydrate at Low Temperatures | Zendy

Hodorowicz S. A. | Zendy; Hodorowicz E. K. | Zendy; Lasocha W. | Zendy; Sagnowski S. | Zendy

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1 H‐NMR and IR Investigations of Phase Situation in Solid Sodium‐Tetramethylammonium Decamolybdate 3.5‐Hydrate at Low Temperatures

Author(s) -

Hodorowicz S. A.,

Hodorowicz E. K.,

Lasocha W.,

Sagnowski S.

Publication year - 1986

Publication title -

crystal research and technology

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.377

H-Index - 64

eISSN - 1521-4079

pISSN - 0232-1300

DOI - 10.1002/crat.2170210412

Subject(s) - tetramethylammonium , hydrate , chemistry , phase (matter) , sodium , atmospheric temperature range , phase transition , proton , nuclear magnetic resonance , inorganic chemistry , ion , organic chemistry , thermodynamics , physics , quantum mechanics

Sodium‐tetramethylammonium decamolybdate 3.5‐hydrate was investigated in the range of 77 to 293 K by X‐ray diffractometric and wide‐line proton magnetic resonance and IR techniques. At low temperatures the compound undergoes transitions connected with change of reorientations of CH 3 , H 2 O and (CH 3 ) 4 N + groups.

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