Cyclic Utilization of Zinc Borate Mother Solution via a New Method | Zendy

Liu Xin | Zendy; Dong Yaping | Zendy; Nai Xueying | Zendy; Wei Ming | Zendy; Li Wu | Zendy

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Cyclic Utilization of Zinc Borate Mother Solution via a New Method

Author(s) -

Liu Xin,

Dong Yaping,

Nai Xueying,

Wei Ming,

Li Wu

Publication year - 2018

Publication title -

crystal research and technology

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.377

H-Index - 64

eISSN - 1521-4079

pISSN - 0232-1300

DOI - 10.1002/crat.201700225

Subject(s) - boron , zinc , octahedron , whisker , depolymerization , zinc borate , chemistry , crystallography , nuclear chemistry , materials science , polymer chemistry , crystal structure , metallurgy , organic chemistry , raw material

Zinc borate mother solution is cycled to prepare 2ZnO·3B 2 O 3 ·7H 2 O, 3ZnO·5B 2 O 3 ·14H 2 O, and 4ZnO·B 2 O 3 ·H 2 O based on the properties of borate depolymerization. The results show uniform quadrilateral‐prism‐like and octahedron‐like 2ZnO·3B 2 O 3 ·7H 2 O are synthesized at different temperatures. Flake‐like 3ZnO·5B 2 O 3 ·14H 2 O is fabricated as reaction time prolonging, and 2ZnO·3B 2 O 3 ·7H 2 O changed into 3ZnO·5B 2 O 3 ·14H 2 O spontaneously. Meanwhile, resulting 2ZnO·3B 2 O 3 ·7H 2 O is investigated to fabricate high aspect ratio of 4ZnO·B 2 O 3 ·H 2 O whisker. Impressively, uniform 4ZnO·B 2 O 3 ·H 2 O whisker can be resynthesized by the filtrates of 2ZnO·3B 2 O 3 ·7H 2 O and 3ZnO·5B 2 O 3 ·14H 2 O via the zero‐waste technology.

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