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Large‐scale synthesis of submicron gallium oxide hydrate rods and their optical and electrochemical properties
Author(s) -
Pei L. Z.,
Yang L. J.,
Dong Y. P.,
Wang J. F.,
Fan C. G.,
Wang S. B.,
Chen J.,
Yin W. Y.,
Zhang Q.F.
Publication year - 2010
Publication title -
crystal research and technology
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.377
H-Index - 64
eISSN - 1521-4079
pISSN - 0232-1300
DOI - 10.1002/crat.201000278
Subject(s) - nanorod , rod , materials science , electrochemistry , hydrothermal circulation , nanotechnology , hydrate , ascorbic acid , gallium , oxide , chemical engineering , chemistry , metallurgy , organic chemistry , electrode , medicine , alternative medicine , food science , pathology , engineering
Large‐scale submicron gallium oxide hydrate (GaOOH) rods have been synthesized by a simple hydrothermal process and their optical, electrochemical properties have been analyzed. The diameter of the GaOOH nanorods with good single crystalline structure is 80‐800 nm and length of less than 4 μm. The tips of the GaOOH structures are composed of nanorods with the diameter of less than 10 nm and length of more than 100 nm. Hydrothermal temperature, time and the Ga‐contained starting materials have important roles on the formation and growth of submicron GaOOH rods. The submicron GaOOH rods exhibit good UV‐vis absorption ability. The electrochemical analysis shows that the submicron GaOOH rods have good detecting ability for ascorbic acid and cysteine in PBS and NaCl solution exhibiting promising potential for electrochemical sensing application. (© 2010 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)