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Growth and characterization of semiorganic NLO crystals of LAHClBr
Author(s) -
Thomas P. C.,
Aruna S.,
Anuradha A.,
Packiam Julius J.,
Arul Pragasam A. Joseph,
Sagayaraj P.
Publication year - 2006
Publication title -
crystal research and technology
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.377
H-Index - 64
eISSN - 1521-4079
pISSN - 0232-1300
DOI - 10.1002/crat.200610755
Subject(s) - dielectric , raman spectroscopy , aqueous solution , evaporation , materials science , characterization (materials science) , analytical chemistry (journal) , crystal growth , single crystal , crystal (programming language) , absorption (acoustics) , crystallography , chemistry , optics , nanotechnology , optoelectronics , organic chemistry , thermodynamics , programming language , physics , computer science , composite material
Single crystals of non‐linear optical (NLO) LAHClBr were grown by slow evaporation technique from its aqueous solution. Good optical quality crystals having dimensions up to 12 × 9 × 7 mm 3 were obtained. The lattice parameters and morphology for the grown crystals were determined using single crystal XRD. The crystals were characterized by FT‐Raman, optical absorption, thermal (DTA and TGA) and dielectric studies. LAHClBr was found to be thermally stable up to 124.3°C. (© 2006 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)