Crystal structure analysis of N,N′‐bis(salicylidene)‐2‐methyl‐1,2‐propanediaminato‐nickel(II) | Zendy

Arıcı C. | Zendy; Ülkü D. | Zendy; Atakol O. | Zendy; Svoboda I. | Zendy; Fuess H. | Zendy

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Crystal structure analysis of N,N′‐bis(salicylidene)‐2‐methyl‐1,2‐propanediaminato‐nickel(II)

Author(s) -

Arıcı C.,

Ülkü D.,

Atakol O.,

Svoboda I.,

Fuess H.

Publication year - 2006

Publication title -

crystal research and technology

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.377

H-Index - 64

eISSN - 1521-4079

pISSN - 0232-1300

DOI - 10.1002/crat.200510578

Subject(s) - orthorhombic crystal system , nickel , crystallography , chemistry , molecule , crystal structure , ligand (biochemistry) , atom (system on chip) , stereochemistry , coordination geometry , crystal (programming language) , ion , hydrogen bond , biochemistry , receptor , organic chemistry , computer science , programming language , embedded system

In the title compound, N,N′‐Bis(salicylidene)‐2‐methyl‐1,2‐propanediaminato‐nickel(II), [NiC 18 H 18 N 2 O 2 ], (CCDC 235278), the Ni II atom is coordinated by two iminic N and two phenolic O atoms of the N,N′‐Bis(salicylidene)‐2‐methyl‐1,2‐propanediaminate (SALPD 2‐ ) ligand. The geometry of the coordination sphere around the Ni atom is distorted square‐planar. Ni(II) ion, forms crystals which belong to the orthorhombic system, space group P cab, with unit cell dimensions a=11.5531(1), b=15.985(4), c=17.418(1) Å, V=3210.5(9) Å 3 . The cell contains eight molecules. The contact distance Ni...Ni a between the neighbouring molecules is 4.4704(8) Å. © 2006 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim

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