Single crystal preparation of Mn  x  Cr 3– x  O 4  by flux method | Zendy

Nevřiva M. | Zendy

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Single crystal preparation of Mn x Cr 3– x O 4 by flux method

Author(s) -

Nevřiva M.

Publication year - 1971

Publication title -

kristall und technik

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.377

H-Index - 64

eISSN - 1521-4079

pISSN - 0023-4753

DOI - 10.1002/crat.19710060408

Subject(s) - flux (metallurgy) , flux method , chromite , crystallography , materials science , analytical chemistry (journal) , crystal (programming language) , mineralogy , single crystal , chemistry , metallurgy , chromatography , computer science , programming language

Mn x Cr 3 x O 4 was prepared by the flux method. Melts of PbOPbF 2 , Bi 2 O 3 B 2 O 3 , B 2 O 3 , Na 2 B 4 O 7 , and Na 2 W 2 O 7 Na 2 WO 4 were used. The best results could be yielded with the PbOPbF 2 flux, from which crystals with 2–4 mm in thickness were grown. The Bi 2 O 3 B 2 O 3 flux produced crystals with 1–2 mm in thickness. The spinell structure of the chromite was proved by X‐ray investigation.

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