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3D Micropatterned All‐Flexible Microfluidic Platform for Microwave‐Assisted Flow Organic Synthesis
Author(s) -
Hur Deniz,
Say Mehmet G.,
Diltemiz Sibel E.,
Duman Fatma,
Ersöz Arzu,
Say Rıdvan
Publication year - 2018
Publication title -
chempluschem
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.801
H-Index - 61
ISSN - 2192-6506
DOI - 10.1002/cplu.201700440
Subject(s) - microfluidics , chemistry , inkwell , nanotechnology , microwave , microwave irradiation , 3d printed , scanning electron microscope , microreactor , chemical engineering , materials science , organic chemistry , composite material , biomedical engineering , medicine , physics , engineering , quantum mechanics , catalysis
A large‐area, all‐flexible, microwaveable polydimethoxysilane microfluidic reactor was fabricated by using a 3D printing system. The sacrificial microchannels were printed on polydimethoxysilane substrates by a direct ink writing method using water‐soluble Pluronic F‐127 ink and then encapsulated between polydimethoxysilane layers. The structure of micron‐sized channels was analyzed by optical and electron microscopy techniques. The fabricated flexible microfluidic reactors were utilized for the acetylation of different amines under microwave irradiation to obtain acetamides in shorter reaction times and good yields by flow organic synthesis.