Inhomogeneous Phase Transition upon Hydrogenation of Nanocluster Pd Films | Zendy

Di Vece Marcel | Zendy; Kelly John J. | Zendy; Lievens Peter | Zendy

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Inhomogeneous Phase Transition upon Hydrogenation of Nanocluster Pd Films

Author(s) -

Di Vece Marcel,

Kelly John J.,

Lievens Peter

Publication year - 2009

Publication title -

chemphyschem

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.016

H-Index - 140

eISSN - 1439-7641

pISSN - 1439-4235

DOI - 10.1002/cphc.200800679

Subject(s) - nanoclusters , palladium , hydrogen , miscibility , materials science , spinodal decomposition , phase (matter) , electrochemistry , chemical engineering , chemical physics , nanotechnology , chemistry , organic chemistry , catalysis , polymer , electrode , engineering , composite material

Phased out: A combination of electrochemical and optical techniques is used to study the interaction of hydrogen with palladium nanoclusters. Hydrogen pressure‐composition isotherms reveal the reduced presence of the β phase in palladium nanoclusters. Hydrogen extraction transients relate the reduced miscibility gap to a core‐shell phase transformation in the palladium nanoclusters (see picture).

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