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13 C– 13 C Chemical Shift Correlation in Rotating Solids without 1 H Decoupling During Mixing
Author(s) -
Herbst Christian,
Riedel Kerstin,
Leppert Jörg,
Ohlenschläger Oliver,
Görlach Matthias,
Ramachandran Ramadurai
Publication year - 2007
Publication title -
chemphyschem
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.016
H-Index - 140
eISSN - 1439-7641
pISSN - 1439-4235
DOI - 10.1002/cphc.200700234
Subject(s) - mixing (physics) , decoupling (probability) , physics , chemistry , atomic physics , analytical chemistry (journal) , quantum mechanics , control engineering , engineering , chromatography
Adiabatic RF pulse schemes using inversion pulses with low power factor are difficult to implement but are shown to be feasible and advantageous for generating 13 C– 13 C MAS solid‐state NMR chemical shift correlation spectra via longitudinal magnetisation exchange without 1H decoupling during mixing (see figure).
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