Premium
Synthesis, Crystal Structure of the Receptor Derived from Diethoxycarbonyl Glycoluril for Aromatic Amide Guest
Author(s) -
Zhou Baohan,
Xu Baoming,
Ma Li,
Wang Meixi,
Chen Kun,
Chen Yanguo
Publication year - 2014
Publication title -
chinese journal of chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.28
H-Index - 41
eISSN - 1614-7065
pISSN - 1001-604X
DOI - 10.1002/cjoc.201400477
Subject(s) - chemistry , amide , monomer , crystallography , aromaticity , single crystal , proton nmr , crystal structure , crystal (programming language) , diffraction , receptor , stereochemistry , molecule , organic chemistry , polymer , biochemistry , computer science , programming language , physics , optics
Abstract The receptor derived from the diethoxycarbonyl glycoluril was synthesized and characterized by IR, 1 H NMR, MS techniques and X‐ray single crystal analysis. Single crystal X‐ray diffraction reveals that the receptor remains monomeric because of its bulky t ‐Bu groups on the side walls. Its unique binding properties for aromatic amides were studied through 1 H NMR and IR techniques.