Absolute Configuration of the Phenylpropanoid Isolated from  Peperomia tetraphylla | Zendy

Yu Yanchao | Zendy; Lu Xiaowei | Zendy; Wu Wenju | Zendy; Wu Yikang | Zendy; Liu Bo | Zendy

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Absolute Configuration of the Phenylpropanoid Isolated from Peperomia tetraphylla

Author(s) -

Yu Yanchao,

Lu Xiaowei,

Wu Wenju,

Wu Yikang,

Liu Bo

Publication year - 2013

Publication title -

chinese journal of chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.28

H-Index - 41

eISSN - 1614-7065

pISSN - 1001-604X

DOI - 10.1002/cjoc.201300648

Subject(s) - enantiopure drug , chemistry , phenylpropanoid , absolute configuration , stereochemistry , organic chemistry , catalysis , enantioselective synthesis , biosynthesis , enzyme

A recently identified phenylpropanoid isolated from Peperomia tetraphylla was synthesized in enantiopure forms using an aldol condensation of enantiopure ( R )‐ N ‐acetyl 4‐phenyl‐oxazolidin‐2‐one as the key step. With the aid of the single crystal X‐ray crystallographic analysis of the synthetic sample, the configuration for the natural product was unambiguously established. Corrected/updated 13 C NMR and optical rotation are also presented.

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