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Preparation of Graphene‐ZnS Nanocomposites via Hydrothermal Method Using Two Sulfide Sources
Author(s) -
Shen Chenfei,
Zheng Mingbo,
Xue Luping,
Li Nianwu,
Lü Hongling,
Zhang Songtao,
Cao Jieming
Publication year - 2011
Publication title -
chinese journal of chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.28
H-Index - 41
eISSN - 1614-7065
pISSN - 1001-604X
DOI - 10.1002/cjoc.201190146
Subject(s) - graphene , hydrothermal circulation , nanocomposite , transmission electron microscopy , chemistry , scanning electron microscope , sulfide , photoluminescence , chemical engineering , hydrothermal synthesis , nanotechnology , analytical chemistry (journal) , materials science , composite material , optoelectronics , organic chemistry , engineering
Graphene‐ZnS nanocomposites were prepared by hydrothermal method using functionalized graphene sheets (FGS) as matrix with Na 2 S and thioacetamide (TAA) as sulfide sources, respectively. The X‐ray diffraction (XRD) patterns reveal that face‐centered cubic ZnS was obtained. The scanning electron microscopy (SEM) and transmission electron microscopy (TEM) results demonstrate different morphological characteristics of the two samples. The optical behaviors of both samples were examined by means of photoluminescence (PL) spectroscopy. The different effects of the two sulfide sources on the formation of the nanocomposites were also discussed to explain the reasons for the differences of morphological characteristics and optical behaviors between two samples.

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