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Synthesis and Insecticidal Activities of 1,3,5‐Trisubstituted‐1,3,5‐hexahydrotriazine‐2‐ N ‐nitroimines
Author(s) -
Xue Sijia,
Ma Xubo,
Bu Hongfei,
Liu Li,
Xu Xiao
Publication year - 2011
Publication title -
chinese journal of chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.28
H-Index - 41
eISSN - 1614-7065
pISSN - 1001-604X
DOI - 10.1002/cjoc.201180373
Subject(s) - chemistry , bioassay , neonicotinoid , stereochemistry , elemental analysis , proton nmr , combinatorial chemistry , organic chemistry , pesticide , imidacloprid , agronomy , genetics , biology
A new series of 1,3,5‐trisubstituted‐1,3,5‐hexahydrotriazine‐2‐ N ‐nitroimines ( 3a – 3j ) were designed and synthesized as novel neonicotinoid analogues, and their structures were characterized by 1 H NMR, IR, elemental analysis and MS. The preliminary bioassay tests showed that most of the target compounds had good insecticidal activities against Nilaparvata lugens as well as Aphis medicaginis at 500 mg/L, while compound 3i had 100% mortality against Nilaparvata lugens at 20 mg/L.