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One‐pot Synthesis of 10‐Methyl‐1,2,3,4,5,6,7,8,9,10‐decahydroacridine‐1,8‐dione Derivatives under Microwave Heating without Catalyst
Author(s) -
Hua GuoPing,
Zhang XiaoJing,
Shi Feng,
Tu ShuJiang,
Xu JiaNing,
Wang Qian,
Zhu XiaoTong,
Zhang JinPeng,
Ji ShunJun
Publication year - 2005
Publication title -
chinese journal of chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.28
H-Index - 41
eISSN - 1614-7065
pISSN - 1001-604X
DOI - 10.1002/cjoc.200591646
Subject(s) - dimedone , chemistry , catalysis , aldehyde , methylamine , microwave heating , organic chemistry , microwave , environmentally friendly , reaction conditions , physics , quantum mechanics , ecology , biology
A series of 10‐methyl‐1,2,3,4,5,6,7,8,9,10‐decahydroacridine‐1,8‐dione derivatives were synthesized by one‐pot reaction of aldehyde, dimedone or 1,3‐cyclohexanedione and methylamine in glycol or water under microwave heating without catalyst. The method has the advantage of short routine and reaction time, high yields as well as friendly environment. And the reaction was not only suitable for aliphatic and aromatic monoaldehyde, but also for aromatic dialdehyde.