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One‐step Solid‐state Synthesis and Characterization of Two Kinds of ZnC 2 O 4 ·2H 2 O Hollow Nanostructures
Author(s) -
YaLi Cao,
Lang Liu,
DianZeng Jia,
XinQuan Xin
Publication year - 2005
Publication title -
chinese journal of chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.28
H-Index - 41
eISSN - 1614-7065
pISSN - 1001-604X
DOI - 10.1002/cjoc.200590539
Subject(s) - chemistry , high resolution transmission electron microscopy , oxalic acid , oxalate , zinc , nanostructure , nuclear chemistry , solid state , chemical engineering , nanotechnology , inorganic chemistry , transmission electron microscopy , organic chemistry , materials science , engineering
Two kinds of zinc oxalate dihydrate (ZnC 2 O 4 ·2H 2 O) hollow nanostructures were synthesized successfully by a simple one‐step solid‐state reaction. ZnC 2 O 4 ·2H 2 O hollow nanospheres were obtained via grinding zinc acetate and oxalic acid, while ZnC 2 O 4 ·2H 2 O hollow nanochains were generated by the analogous reaction under the presence of a surfactant PEG 400. The as‐prepared samples were characterized by XRD, TEM, HRTEM, SEM, IR and TG/DTA