Hydrothermal Synthesis and Structure of K 3 Na 5 (H 2 NCH 2 CH 2 NH 3 ) 2 {(VO) 12 O 6 [B 3 O 6 (OH)] 6 }(H 2 O)·12H 2 O | Zendy

Bin Lu | Zendy; Hong Wang | Zendy; Li Zhang | Zendy; ChengYong DAI | Zendy; QingHai Cai | Zendy; YongKui Shan | Zendy

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Hydrothermal Synthesis and Structure of K 3 Na 5 (H 2 NCH 2 CH 2 NH 3 ) 2 {(VO) 12 O 6 [B 3 O 6 (OH)] 6 }(H 2 O)·12H 2 O

Author(s) -

Bin Lu,

Hong Wang,

Li Zhang,

ChengYong DAI,

QingHai Cai,

YongKui Shan

Publication year - 2005

Publication title -

chinese journal of chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.28

H-Index - 41

eISSN - 1614-7065

pISSN - 1001-604X

DOI - 10.1002/cjoc.200590137

Subject(s) - monoclinic crystal system , chemistry , crystallography , hydrothermal synthesis , crystal structure , molecule , ion , x ray crystallography , group (periodic table) , center (category theory) , hydrothermal circulation , stereochemistry , diffraction , physics , organic chemistry , optics , seismology , geology

A new compound containing polyoxovanadoborate anion was synthesized and characterized by single‐crystal X‐ray diffraction analysis. A water molecule at the center of the anion was precisely determined. The crystals of the new compound belong to the monoclinic system, space group P2 1 / n with a =1.35002(7), b =2.0864(1), c =2.3667(1) nm, β=90.669(1)°, V =6.6660(5) nm 3 , Z =4, µ=2.066 mm −1 , D c =2.352 g/cm 3 , M r =2359.2, S =1.152, R =0.0642, wR =0.0789.

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