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Intermolecular Phenolic Hydroxy Methylation Occurring between Chiral N,N′ ‐Bis(2‐hydroxyphenyl)‐2,2‐dimethyl‐1,3‐dioxolane‐4,5‐dicarbamide and Co‐crystallized Methanol under Electron Impact Ionization Conditions
Author(s) -
Xu JiaXi,
Jiao Peng,
He Zheng,
Zhang QiHan,
Yan ChunHua
Publication year - 2004
Publication title -
chinese journal of chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.28
H-Index - 41
eISSN - 1614-7065
pISSN - 1001-604X
DOI - 10.1002/cjoc.20040220513
Subject(s) - chemistry , dioxolane , methanol , intermolecular force , electron ionization , enantiomer , dimethyl ether , methylation , ionization , medicinal chemistry , crystallography , organic chemistry , molecule , ion , biochemistry , gene
An intermolecular phenolic hydroxy methylation occurring between chiral N,N′ ‐bis(2‐hydroxyphenyl)‐2,2‐dimethyl‐1,3‐dioxolane‐4,5dicarbamide and co‐crystallized methanol under electron impact ionization conditions was observed. The result was confirmed by X‐ray diffraction structural analysis of a co‐crystalline of ( R,R )‐enantiomer and methanol.