Synthesis, crystal structures and characterization of Ba 5 LiTiNb 9 O 30 | Zendy

Liu HanXing | Zendy; Zou Long | Zendy; Zhou Jian | Zendy; Fang Liang | Zendy; Zhang GaoKe | Zendy; Ouyang ShiXi | Zendy

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Synthesis, crystal structures and characterization of Ba 5 LiTiNb 9 O 30

Author(s) -

Liu HanXing,

Zou Long,

Zhou Jian,

Fang Liang,

Zhang GaoKe,

Ouyang ShiXi

Publication year - 2004

Publication title -

chinese journal of chemistry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.28

H-Index - 41

eISSN - 1614-7065

pISSN - 1001-604X

DOI - 10.1002/cjoc.20040220508

Subject(s) - chemistry , tetragonal crystal system , crystal structure , scanning electron microscope , microstructure , crystallography , tungsten , doping , characterization (materials science) , chemical formula , analytical chemistry (journal) , nanotechnology , materials science , optoelectronics , organic chemistry , chromatography , composite material

A new niobate compound with the chemical composition of Ba 5 LiTiNb 9 O 30 was synthesized by doping Li + into the system BaO‐TiO 2 ‐Nb 2 O 5 in conventional solid state reaction method. The crystalline structure was determined by X‐ray dilation analysis (XRD). The results showed that crystal structure of Ba 5 LiTiNb 9 O 30 belongs to tetragonal tungsten bronze structure with space group P4 bm and its unit cell parameters: a=b= 1.2512(2) nm, c= 0.4008(5) nm. The microstructure of reaction products was observed by scanning electron microscopy (SEM).

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