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Direct synthesis of 3‐fluoroalkyl‐2,6‐diethoxycarbonyl phenols
Author(s) -
HuiPing Guan,
QiaoSheng Hu,
ChangMing Hu
Publication year - 1996
Publication title -
chinese journal of chemistry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.28
H-Index - 41
eISSN - 1614-7065
pISSN - 1001-604X
DOI - 10.1002/cjoc.19960140115
Subject(s) - phenols , chemistry , aldehyde , organic chemistry , alkyl , phenol , catalysis
Cyclocondensation of α‐fluoroalkyl ketones or α‐fluoroalkyl aldehyde (1) and diethyl 1,3‐acetonedicarboxylate (2) affords 3‐fluoroalkyl‐2,6‐diethoxycarbonyl‐5‐alkyl‐phenols (3) in good yields. This provides a novel method for the preparation of meta‐fluoroalkyl polysubstituted phenols.