Open metallocenes: VII. The syntheses and low temperature X‐ray diffraction analyses of bis‐(2,4‐dimethylpentadienyl)‐vanadium monocarbonyl | Zendy

GuangDi Yang | Zendy; JuZheng Liu | Zendy; YuQuo Fan | Zendy; YingQiu Liang | Zendy

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Open metallocenes: VII. The syntheses and low temperature X‐ray diffraction analyses of bis‐(2,4‐dimethylpentadienyl)‐vanadium monocarbonyl

Author(s) -

GuangDi Yang,

JuZheng Liu,

YuQuo Fan,

YingQiu Liang

Publication year - 1987

Publication title -

acta chimica sinica english edition

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.28

H-Index - 41

eISSN - 1614-7065

pISSN - 0256-7660

DOI - 10.1002/cjoc.19870050202

Subject(s) - chemistry , orthorhombic crystal system , crystallography , metallocene , vanadium , diffraction , crystal structure , x ray crystallography , stereochemistry , inorganic chemistry , organic chemistry , physics , optics , polymerization , polymer

An open metallocene compound, [2,4‐(CH 3 ) 2 C 5 H 5 ] 2 VCO has been synthesized and characterized by a low temperature (‐60°C) X‐ray diffraction technique. The compound crystallizes in an orthorhombic space group P 2 1 2 1 2 1 with lattice parameters a =9.921(6), b =9.899(6), c =14.491(8) Å, Z =4. The structure was refined by the block‐matrix least‐squares the final R =0.087

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