Facile Diastereoseparation of Glycosyl Sulfoxides by Chiral Stationary Phase | Zendy

Taniguchi Tohru | Zendy; Asahata Mai | Zendy; Nasu Akihito | Zendy; Shichibu Yukatsu | Zendy; Konishi Katsuaki | Zendy; Monde Kenji | Zendy

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Facile Diastereoseparation of Glycosyl Sulfoxides by Chiral Stationary Phase

Author(s) -

Taniguchi Tohru,

Asahata Mai,

Nasu Akihito,

Shichibu Yukatsu,

Konishi Katsuaki,

Monde Kenji

Publication year - 2016

Publication title -

chirality

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.43

H-Index - 77

eISSN - 1520-636X

pISSN - 0899-0042

DOI - 10.1002/chir.22610

Subject(s) - chemistry , glycosyl , phase (matter) , chiral stationary phase , combinatorial chemistry , organic chemistry , computational chemistry

Separation of the diastereomers of glycosyl sulfoxides differing in the sulfur chirality has been difficult. This article presents a fast and scalable method for their diastereoseparation using a chiral stationary phase. The usefulness of this method was demonstrated in a 500‐mg scale separation within 20 min, and in the separation of trisaccharyl sulfoxide diastereomers. Chirality 28:534–539, 2016 . © 2016 Wiley Periodicals, Inc.

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