Resolution and absolute configuration assignment of a chiral hemicryptophane molecular cage | Zendy

Perraud Olivier | Zendy; Raytchev Pascal Dimitrov | Zendy; Martinez Alexandre | Zendy; Dutasta JeanPierre | Zendy

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Resolution and absolute configuration assignment of a chiral hemicryptophane molecular cage

Author(s) -

Perraud Olivier,

Raytchev Pascal Dimitrov,

Martinez Alexandre,

Dutasta JeanPierre

Publication year - 2010

Publication title -

chirality

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.43

H-Index - 77

eISSN - 1520-636X

pISSN - 0899-0042

DOI - 10.1002/chir.20876

Subject(s) - chemistry , absolute configuration , enantiomer , circular dichroism , cage , chiral stationary phase , resolution (logic) , chiral column chromatography , stereochemistry , chromatography , mathematics , combinatorics , artificial intelligence , computer science

The racemic hemicryptophane molecular cage 2 was resolved by semipreparative HPLC on Whelk‐O1 column. The absolute configuration of each isolated enantiomer was established from the analysis of their circular dichroism spectra and assigned as P ‐(+)‐ 2 and M ‐(−)‐ 2 . Chirality, 2010. © 2010 Wiley‐Liss, Inc.

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