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Gas–Liquid Segmented Flow Microfluidics for Screening Pd‐Catalyzed Carbonylation Reactions
Author(s) -
Gong Xiuqing,
Miller Philip W.,
Gee Antony D.,
Long Nicholas J.,
de Mello Andrew J.,
Vilar Ramon
Publication year - 2012
Publication title -
chemistry – a european journal
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.687
H-Index - 242
eISSN - 1521-3765
pISSN - 0947-6539
DOI - 10.1002/chem.201104059
Subject(s) - carbonylation , catalysis , flow (mathematics) , microfluidics , chemistry , computer science , combinatorial chemistry , nanotechnology , organic chemistry , materials science , physics , mechanics , carbon monoxide
Go with the (segmented) flow : A gas–liquid microfluidic reactor system has been developed to study Pd‐catalyzed carbonylation reactions over a range of flow regimes and reaction conditions (see picture). The segmented gas–liquid flow regime, in comparison to annular flow, enables reactions to be studied over longer reaction times and without the buildup of unwanted Pd particles.