A Convenient Synthesis and a NMR Study of the Diammoniate of Diborane | Zendy

Lingam Hima K. | Zendy; Chen Xuenian | Zendy; Zhao JiCheng | Zendy; Shore Sheldon G. | Zendy

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A Convenient Synthesis and a NMR Study of the Diammoniate of Diborane

Author(s) -

Lingam Hima K.,

Chen Xuenian,

Zhao JiCheng,

Shore Sheldon G.

Publication year - 2012

Publication title -

chemistry – a european journal

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.687

H-Index - 242

eISSN - 1521-3765

pISSN - 0947-6539

DOI - 10.1002/chem.201103693

Subject(s) - diborane , borohydride , chemistry , boranes , metathesis , nuclear magnetic resonance spectroscopy , cyclopentanes , nmr spectra database , organic chemistry , spectral line , boron , physics , catalysis , polymerization , polymer , astronomy

DADB synthesis : The diammoniate of diborane (DADB) was synthesized in a new metathesis reaction between the diammoniate of monochloroborane and potassium borohydride in liquid ammonia (see scheme). 1 H and 11 B NMR spectra of DADB are reported. The stability in THF was examined by variable‐temperature 11 B NMR spectroscopy.

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