BDPA: An Efficient Polarizing Agent for Fast Dissolution Dynamic Nuclear Polarization NMR Spectroscopy | Zendy

Lumata Lloyd | Zendy; Ratnakar S. James | Zendy; Jindal Ashish | Zendy; Merritt Matthew | Zendy; Comment Arnaud | Zendy; Malloy Craig | Zendy; Sherry A. Dean | Zendy; Kovacs Zoltan | Zendy

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BDPA: An Efficient Polarizing Agent for Fast Dissolution Dynamic Nuclear Polarization NMR Spectroscopy

Author(s) -

Lumata Lloyd,

Ratnakar S. James,

Jindal Ashish,

Merritt Matthew,

Comment Arnaud,

Malloy Craig,

Sherry A. Dean,

Kovacs Zoltan

Publication year - 2011

Publication title -

chemistry – a european journal

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.687

H-Index - 242

eISSN - 1521-3765

pISSN - 0947-6539

DOI - 10.1002/chem.201102037

Subject(s) - dissolution , nuclear magnetic resonance spectroscopy , polarization (electrochemistry) , spectroscopy , chemistry , materials science , chemical engineering , organic chemistry , physics , quantum mechanics , engineering

Teaching an old free radical new tricks : The stable free radical 1,3‐bisdiphenylene‐2‐phenylallyl (BDPA) is an efficient polarizing agent in the dissolution dynamic nuclear polarization (DNP) of a variety of hydrophilic and hydrophobic compounds, such as tetramethylallene or [ 15 N]choline (see figure). In addition, BDPA can be easily removed from the hyperpolarized solution by a simple mechanical filtration, when water is used for dissolution.

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