In Situ Generation and Intramolecular Schmidt Reaction of Keto Azides in a Microwave‐Assisted Flow Format | Zendy

Painter Thomas O. | Zendy; Thornton Paul D. | Zendy; Orestano Mario | Zendy; Santini Conrad | Zendy; Organ Michael G. | Zendy; Aubé Jeffrey | Zendy

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In Situ Generation and Intramolecular Schmidt Reaction of Keto Azides in a Microwave‐Assisted Flow Format

Author(s) -

Painter Thomas O.,

Thornton Paul D.,

Orestano Mario,

Santini Conrad,

Organ Michael G.,

Aubé Jeffrey

Publication year - 2011

Publication title -

chemistry – a european journal

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.687

H-Index - 242

eISSN - 1521-3765

pISSN - 0947-6539

DOI - 10.1002/chem.201100768

Subject(s) - intramolecular force , trifluoroacetic acid , microwave irradiation , microwave , computer science , combinatorial chemistry , flow (mathematics) , in situ , chemistry , stereochemistry , organic chemistry , mathematics , telecommunications , geometry

Go with the flow! A method for conversion of keto halides to lactams by means of sequential azidation and intramolecular Schmidt reaction in a combined flow format is described (see scheme; MWI=microwave irradiation, TFA=trifluoroacetic acid).

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