Residual Dipolar Couplings (RDCs) Analysis of Small Molecules Made Easy: Fast and Tuneable Alignment by Reversible Compression/Relaxation of Reusable PMMA Gels | Zendy

Gayathri Chakicherla | Zendy; Tsarevsky Nicolay V. | Zendy; Gil Roberto R. | Zendy

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Residual Dipolar Couplings (RDCs) Analysis of Small Molecules Made Easy: Fast and Tuneable Alignment by Reversible Compression/Relaxation of Reusable PMMA Gels

Author(s) -

Gayathri Chakicherla,

Tsarevsky Nicolay V.,

Gil Roberto R.

Publication year - 2010

Publication title -

chemistry – a european journal

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.687

H-Index - 242

eISSN - 1521-3765

pISSN - 0947-6539

DOI - 10.1002/chem.200903378

Subject(s) - relaxation (psychology) , isotropy , anisotropy , residual dipolar coupling , dipole , residual , compression (physics) , molecule , materials science , computer science , combinatorial chemistry , chemistry , physics , algorithm , organic chemistry , optics , composite material , psychology , social psychology

Tuneable RDCs : A fast and tunable method for measuring anisotropic NMR parameters using variable compression/relaxation of clean and reusable PMMA gels in CDCl 3 is introduced (see picture). No special devices are needed. The configuration and conformation of small molecules can be determined by using the RDC slopes without the need for performing a control experiment in isotropic conditions.

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