The Synthesis, Full Characterisation and Utilisation of Template‐Free Silica Sodalite, a Novel Polymorph of Silica | Zendy

King R. S. P. | Zendy; Dann S. E. | Zendy; Elsegood M. R. J. | Zendy; Kelly P. F. | Zendy; Mortimer R. J. | Zendy

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The Synthesis, Full Characterisation and Utilisation of Template‐Free Silica Sodalite, a Novel Polymorph of Silica

Author(s) -

King R. S. P.,

Dann S. E.,

Elsegood M. R. J.,

Kelly P. F.,

Mortimer R. J.

Publication year - 2009

Publication title -

chemistry – a european journal

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 1.687

H-Index - 242

eISSN - 1521-3765

pISSN - 0947-6539

DOI - 10.1002/chem.200802551

Subject(s) - sodalite , ethylene glycol , materials science , atmosphere (unit) , crystallization , chemical engineering , ethylene , crystallography , zeolite , chemistry , organic chemistry , catalysis , thermodynamics , physics , engineering

Empty glass : Subjecting ethylene glycol silica sodalite to heat (680 °C) under a nitrogen atmosphere (i) successfully removes the templating agent to give cubic silica sodalite, which, upon consequent heating under an oxygen atmosphere (ii), transforms into a rhombohedral form of the empty sodalite, in effect a novel polymorph of silica.

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