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Microwave‐Assisted Reaction Engineering: Microwave Apparatus at Mini‐Plant Scale with Online Analysis
Author(s) -
Bierbaum R.,
Nüchter M.,
Ondruschka B.
Publication year - 2005
Publication title -
chemical engineering and technology
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.403
H-Index - 81
eISSN - 1521-4125
pISSN - 0930-7516
DOI - 10.1002/ceat.200500045
Subject(s) - microwave , process engineering , scale (ratio) , sampling (signal processing) , scale up , filter (signal processing) , pilot plant , computer science , environmental science , engineering , waste management , telecommunications , electrical engineering , physics , classical mechanics , quantum mechanics
A new mini‐plant setup is described with online HPLC analysis. This setup allows scale up to pilot‐plant scale and will help in transferring the advantages of microwave‐assisted syntheses to a technical scale. Also filter setup options that can be used to protect the analysis system from suspended particles or depositions are described, and show that analysis time is not significantly prolonged by the automated sampling procedure.