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A Microfluidic System for the Continuous Recycling of Unmodified Homogeneous Palladium Catalysts through Liquid/Liquid Phase Separation
Author(s) -
Li Pengfei,
Moore Jason S.,
Jensen Klavs F.
Publication year - 2013
Publication title -
chemcatchem
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 1.497
H-Index - 106
eISSN - 1867-3899
pISSN - 1867-3880
DOI - 10.1002/cctc.201300054
Subject(s) - catalysis , palladium , homogeneous , liquid liquid , microfluidics , liquid phase , phase (matter) , chemical engineering , materials science , homogeneous catalysis , hydroxylation , ionic liquid , chemistry , organic chemistry , chromatography , nanotechnology , thermodynamics , physics , engineering , enzyme
A parting of the waves: A prototype microflow system for the continuous recycling of homogeneous catalysts through liquid/liquid phase separation was developed and its effectiveness demonstrated in a challenging palladium‐catalyzed hydroxylation reaction. The unmodified catalyst is recycled under standard reaction conditions by using a combination of chemical and engineering methods.