Synthesis, Separation and Characterization of Unsymmetrically Substituted Phthalocyanines | Zendy

Linßen Torsten Golo | Zendy; Hanack Michael | Zendy

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Synthesis, Separation and Characterization of Unsymmetrically Substituted Phthalocyanines

Author(s) -

Linßen Torsten Golo,

Hanack Michael

Publication year - 1994

Publication title -

chemische berichte

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.667

H-Index - 136

eISSN - 1099-0682

pISSN - 0009-2940

DOI - 10.1002/cber.19941271030

Subject(s) - chemistry , condensation , nickel , column chromatography , characterization (materials science) , phthalocyanine , nuclear magnetic resonance spectroscopy , spectroscopy , polycyclic compound , polymer chemistry , organic chemistry , stereochemistry , molecule , nanotechnology , physics , materials science , quantum mechanics , thermodynamics

Unsymmetrically substituted (phthalocyaninato)nickel(II) complexes –7 were synthesized by statistical condensation of 4,5‐dipentoxy‐ ( 2a ), 4,5‐diheptyl‐ ( 2b ), 3,6‐dihexoxy‐ ( 2c ), and 3,6‐diheptylphthalonitrile ( 2d ) with 3,4,5,6‐tetraphenylphthalonitrile ( 1 ) and separated by column chromatography. The obtained phthalocyanines 3–7 were characterized by UV‐, IR‐, and 1 H‐NMR spectroscopy.

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