Beiträge zur Chemie des Bors, 206. Darstellung und strukturelle Charakterisierung der  p ‐Formylbenzolboronsäure | Zendy

Feulner Herta | Zendy; Linti Gerald | Zendy; Nöth Heinrich | Zendy

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Beiträge zur Chemie des Bors, 206. Darstellung und strukturelle Charakterisierung der p ‐Formylbenzolboronsäure

Author(s) -

Feulner Herta,

Linti Gerald,

Nöth Heinrich

Publication year - 1990

Publication title -

chemische berichte

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.667

H-Index - 136

eISSN - 1099-0682

pISSN - 0009-2940

DOI - 10.1002/cber.19901230915

Subject(s) - chemistry , triclinic crystal system , tetrahydrofuran , molecule , benzene , stereochemistry , hydrogen bond , group (periodic table) , crystal structure , crystallography , medicinal chemistry , organic chemistry , solvent

Contributions to the Chemistry of Boron, 206. — Preparation and Structural Characterization of p‐Formylbenzeneboronic Acid The Grignard compound prepared from 1‐bromo‐4‐(diethoxymethyl)benzene in tetrahydrofuran reacts with tri‐n‐butoxyborane to produce the title compound in 78% yield after hydrolytic workup. The molecule crystallizes in the triclinic space group P &1bar;, Z 2, its B(OH) 2 group showing extensive intermolecular hydrogen bonding. The formyl group is disordered.

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