Zur Kenntnis des „Phosphormonosulfids”︁ (PS)  x | Zendy

Frehn Angelika | Zendy; Keck Helmut | Zendy; Kuchen Wilhelm | Zendy

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Zur Kenntnis des „Phosphormonosulfids”︁ (PS) x

Author(s) -

Frehn Angelika,

Keck Helmut,

Kuchen Wilhelm

Publication year - 1990

Publication title -

chemische berichte

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.667

H-Index - 136

eISSN - 1099-0682

pISSN - 0009-2940

DOI - 10.1002/cber.19901230620

Subject(s) - chemistry , halogenation , phosphorus , orange (colour) , medicinal chemistry , crystallography , organic chemistry , food science

New Results Concerning the “Phosphorus Monosulfide” (PS) x The orange‐yellow solid of approximate composition (PS) x obtained by dehalogenation of P(S)Br 3 with Mg proved to be a mixture of phosphorus sulfides e.g. P 4 S 3 , P 4 S 4 , P 4 S 5 , P 4 S 7 , and insoluble polymeric material. It is suggested that the latter contains a network of triply connected P atoms, many of which are substituted by groups. The conclusions are based on the results of analytical, mass‐spectrometric and 31 P‐NMR‐spectroscopic findings.

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