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Eine einfache darstellung für S 2 N 2
Author(s) -
Roesky Herbert W.,
Anhaus Jens
Publication year - 1982
Publication title -
chemische berichte
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.667
H-Index - 136
eISSN - 1099-0682
pISSN - 0009-2940
DOI - 10.1002/cber.19821151120
Subject(s) - chemistry , pyrolysis , medicinal chemistry , analytical chemistry (journal) , organic chemistry
A Facile Synthesis of S 2 N 2 The reaction of S 4 N 4 with S 2 N 2 · 2 AlCl 3 ( 1 ) at 80° C in high vacuum results in the formation of S 2 N 2 . The advantage of this method in comparison to the direct pyrolysis of S 4 N 4 at 300°C is the reduction of temperature to 80°C. On safety arguments, S 2 N 2 has now become available on a preparative scale. The spectra of S 2 N 2 · 2 AlCl 3 are discussed.