Capillary column gas chromatographic mass spectrometric analysis of anabolic steroid residues using splitless injections made at elevated temperatures | Zendy

Houghton E. | Zendy; Teale P. | Zendy

Premium

Capillary column gas chromatographic mass spectrometric analysis of anabolic steroid residues using splitless injections made at elevated temperatures

Author(s) -

Houghton E.,

Teale P.

Publication year - 1981

Publication title -

biomedical mass spectrometry

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.475

H-Index - 121

eISSN - 1096-9888

pISSN - 0306-042X

DOI - 10.1002/bms.1200080808

Subject(s) - chemistry , chromatography , mass spectrometry , gas chromatography , capillary action , dodecane , tetradecane , gas chromatography–mass spectrometry , anabolic steroid , urine , boiling , anabolism , nandrolone , vaporization , solvent , organic chemistry , biochemistry , materials science , composite material

The use of capillary column gas chromatography mass spectrometry has been investigated for the detection of the presence of estrane‐3,17α‐diol in horse urine extracts; the detection of this diol confirms the administration of anabolic steroids based upon 19‐nortestosterone. To reduce analysis time, but yet maintain a solvent effect in the splitless injection mode, injections have been made at elevated temperatures (190–220°C) using high boiling solvents (dodecane b.p. 214°C and tetradecane b.p. 252°C).

This content is not available in your region!

Continue researching here.

Having issues? You can contact us here

Accelerating Research