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Gas chromatographic mass spectrometric identification of N ‐dicarboxylmonoglycines
Author(s) -
Gregersen Niels,
Grøn Ida,
Rasmussen Karsten,
Kølvraa Steen
Publication year - 1978
Publication title -
biomedical mass spectrometry
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.475
H-Index - 121
eISSN - 1096-9888
pISSN - 0306-042X
DOI - 10.1002/bms.1200050115
Subject(s) - chromatography , mass spectrum , chemistry , mass spectrometry , methylene , gas chromatography , gas chromatography–mass spectrometry , analytical chemistry (journal) , organic chemistry
Abstract A number of N ‐dicarboxylmonoglycines of biological interest have been synthesized. They were characterized by means of mass spectrometry. Gas chromatography of the methyl esters of methylmalonyl‐, succinyl‐, glutaryl‐, adipyl‐, suberyl‐ and sebacylglycines showed a single sharp peak for each compound on Dexsil 300 and OV 17 columns. Methylene unit values and mass spectra of the six methyl esters are reported.