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A novel series of hybrid molecules  4a – i  and  5a – i  were prepared by condensation of 4‐(trimethylsilylethynyl)benzaldehyde  1  with substituted  o ‐phenylenediamines. These in turn were reacted with 2‐(azidomethoxy)ethyl acetate in a Cu alkyne–azide cycloaddition (CuAAC) to generate the 1,2,3‐triazole pharmacophore under microwave assistance. The newly synthesized compounds were examined for their  in vitro  antimicrobial activities against Gram‐positive and Gram‐negative bacteria and the phytopathogenic fungi  Verticillium dahliae  and  Fusarium oxysporum  f. sp.  albedinis . 2‐((4‐(4‐(5‐Trifluoromethyl benzimidazol‐2‐yl)phenyl)‐1,2,3‐triazol‐1‐yl)methoxy)ethanol  5e  showed a moderate inhibition of 30% in the Foa sporulation test.

Benzimidazole‐1,2,3‐triazole Hybrid Molecules: Synthesis and Evaluation for Antibacterial/Antifungal Activity