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Synthesis and modification of silica‐based epoxy nanocomposites with different sol–gel process enhanced thermal and mechanical properties
Author(s) -
Aziz Tariq,
Mehmood Sahid,
Haq Fazal,
Ullah Roh,
Khan Farman Ullah,
Ullah Bakhtar,
Raheel Muhammad,
Iqbal Mudassir,
Ullah Asmat
Publication year - 2021
Publication title -
journal of applied polymer science
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.575
H-Index - 166
eISSN - 1097-4628
pISSN - 0021-8995
DOI - 10.1002/app.51191
Subject(s) - materials science , nanocomposite , epoxy , thermogravimetric analysis , composite material , fourier transform infrared spectroscopy , x ray photoelectron spectroscopy , surface modification , scanning electron microscope , nanoparticle , chemical engineering , nanotechnology , engineering
This research article describes the results of nano‐silica composites filled with different epoxy contents containing nano‐SiO 2 particles from (5–25 wt%). Reinforcing hybrid composites enhance thermal and mechanical properties to achieve vital and sustainable products. Silica‐based nanocomposites with high purity were prepared and used for the surface modification of nanosized silica particles. The surface structure's composition and physical properties of modified nano‐SiO 2 particles were characterized through Fourier transferred infrared spectrometer, X‐ray photoelectron spectroscopy, thermogravimetric analyzer, and scanning electron microscopic. Silica‐based nanocomposites were prepared by incorporating of modified nano‐SiO 2 as an enhancing filler. The morphology of fracture surface and dynamic mechanical properties were investigated. Results showed that the silica‐based epoxy nanocomposites are bearing a long chain structure that could improve the compatibility of silica nanocomposites with epoxy resin and contribute to a better dispersion state in the matrix, which enhanced the overall performance of epoxy‐cured products.