A molecular imprinted polymer on the surface of superparamagnetic Fe 3 O 4 –graphene oxide (MIP@Fe 3 O 4 @GO) for simultaneous recognition and enrichment of evodiamine and rutaecarpine in  Evodiae fructus | Zendy

Fan JiePing | Zendy; Liao DanDan | Zendy; Xie YanLong | Zendy; Zheng Bing | Zendy; Yu JiaXin | Zendy; Cao YaHui | Zendy; Zhang XueHong | Zendy; Peng HaiLong | Zendy

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A molecular imprinted polymer on the surface of superparamagnetic Fe 3 O 4 –graphene oxide (MIP@Fe 3 O 4 @GO) for simultaneous recognition and enrichment of evodiamine and rutaecarpine in Evodiae fructus

Author(s) -

Fan JiePing,

Liao DanDan,

Xie YanLong,

Zheng Bing,

Yu JiaXin,

Cao YaHui,

Zhang XueHong,

Peng HaiLong

Publication year - 2017

Publication title -

journal of applied polymer science

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.575

H-Index - 166

eISSN - 1097-4628

pISSN - 0021-8995

DOI - 10.1002/app.44465

Subject(s) - superparamagnetism , materials science , molecularly imprinted polymer , graphene , evodiamine , adsorption , fourier transform infrared spectroscopy , oxide , polymer , chemical engineering , nuclear chemistry , analytical chemistry (journal) , selectivity , nanotechnology , chemistry , chromatography , organic chemistry , magnetization , composite material , magnetic field , physics , quantum mechanics , engineering , metallurgy , catalysis

A composite material (MIP@Fe 3 O 4 @GO) based on molecular imprinted polymer (MIP), superparamagnetic Fe 3 O 4 particles and graphene oxide (GO) was prepared by the chemical coprecipitation method, and used to simultaneously separate and enrich two alkaloids (evodiamine and rutaecarpine) in the extract of Evodiae fructus . The as‐prepared MIP@Fe 3 O 4 @GO was characterized by Fourier transform infrared spectroscopy (FT‐IR), transmission electron microscopy (TEM), and vibrating sample magnetometer (VSM). The adsorption kinetics, isotherms, competitive adsorption, and reusability of MIP@Fe 3 O 4 @GO were also investigated. The results revealed that MIP@Fe 3 O 4 @GO was sensitive to the magnetic field and could be easily separated using an external magnet; MIP@Fe 3 O 4 @GO showed good recognition selectivity, as well as simultaneous enrichment and separation abilities for evodiamine and rutaecarpine in the extract of E. fructus with satisfactory recoveries. © 2016 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2017 , 134 , 44465.

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