Tri‐ n ‐Butylborane oxide‐initiated homopolymerization of vinyl monomers containing cyano or isocyanato groups | Zendy

Chappelow Cecil C. | Zendy; Pinzino Charles S. | Zendy; Byerley Thomas J. | Zendy; Eick J. David | Zendy

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Tri‐ n ‐Butylborane oxide‐initiated homopolymerization of vinyl monomers containing cyano or isocyanato groups

Author(s) -

Chappelow Cecil C.,

Pinzino Charles S.,

Byerley Thomas J.,

Eick J. David

Publication year - 1995

Publication title -

journal of applied polymer science

Language(s) - English

Resource type - Journals

SCImago Journal Rank - 0.575

H-Index - 166

eISSN - 1097-4628

pISSN - 0021-8995

DOI - 10.1002/app.1995.070580708

Subject(s) - polymer chemistry , tetrahydrofuran , methacrylate , monomer , chemistry , ethyl acrylate , oxide , radical polymerization , vinyl acetate , methyl methacrylate , copolymer , organic chemistry , polymer , solvent

Homopolymers of 2‐isocyanatoethyl methacrylate, ethyl α‐cyanoacrylate, and ethyl α‐is‐ocyanatoacrylate were prepared in tetrahydrofuran at 22 to 25°C using tri‐ n ‐butylborane oxide as a free radical initiator. Additionally, ethyl α‐isocyanatoacrylate was homopolymerized using 2,2′‐azobis(2‐methylbutyronitrile) as the initiator. Homopolymers were characterized by photoacoustic FT‐IR, DSC, and elemental analysis. © 1995 John Wiley & Sons, Inc.

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