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Study of nylon 6 and poly(propylene oxide) blends by thermal measurements and carbon‐13 NMR high resolution solid‐state
Author(s) -
Tavares Maria Inês Bruno,
Castro Washington P.,
Costa Dilma A.
Publication year - 1995
Publication title -
journal of applied polymer science
Language(s) - English
Resource type - Journals
SCImago Journal Rank - 0.575
H-Index - 166
eISSN - 1097-4628
pISSN - 0021-8995
DOI - 10.1002/app.1995.070550803
Subject(s) - differential scanning calorimetry , materials science , thermogravimetric analysis , magic angle spinning , propylene oxide , oxide , solid state nuclear magnetic resonance , magic angle , analytical chemistry (journal) , polymer chemistry , solid state , nuclear magnetic resonance spectroscopy , polymer , chemistry , nuclear magnetic resonance , composite material , ethylene oxide , copolymer , organic chemistry , thermodynamics , physics , metallurgy
Samples of Nylon 6/poly(propylene oxide), with poly(propylene oxide) (PPO) content varying up to 35%, have been examined using thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), and nuclear magnetic resonance (NMR) carbon‐13 at solid‐state. Carbon‐13 spectra were measured by cross‐polarization (CP), magic angle spinning (MAS), and high‐power hydrogen decoupling (HPHD). The variation contact time experiment and MAS technique were also determined. The data are discussed in terms of compatibility and plasticization of the samples. © 1995 John Wiley & Sons, Inc.